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001704

001704-5g



4-Dimethylaminopyridine


CAS Number: 1122-58-3
   
Molecular Formula: C7H10N2
   
Molecular Weight: 122.17
   
MDL Number: MFCD00006418

Special Handling and Safety: >1 grams air/>500 grams ground - DOT. Special DOT Box Charge $20

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001704-5g
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001704-10g
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001704-25g
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001704-100g
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001704-500g
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001704-1kg
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001704-5Kg
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Purity:98%
Mp:112-114°
 
Pictograms:
Signal Word:Danger
Hazard Statements:H301, H310, H315, H319, H335
Precautionary Statements:P280, P301 + P312, P305 + P351 + P338
UN#:UN2811
Packing Group:II
Hazard Class:6.1
Flash Point:124°
RTECS:US9230000
SDS: See MSDS
 
Limited Quantities:100ml (liquid) or 0.5 Kg (solid)
Excepted Quantities:Max Inner Pack (1g or 1ml) and Max Outer Pack (500g or 500ml)

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DMAP is a useful nucleophilic catalyst for a variety of reactions such as esterifications with anhydrides4, the Baylis-Hillman reaction5, hydrosilylations, tritylation, the Steglich rearrangement and the Staudinger synthesis of β-lactams. Chiral DMAP analogues are used in kinetic resolution experiments of mainly secondary alcohols and Evans auxilary type amides. 1,2  DMAP is also used as a coupling agent for the synthesis of peptide and an efficient ligand for the Heck reaction in aqueous media 3.


Reference
  1. Höfle, G., Steglich, W., Vorbrüggen, H.. Angew. Chem. Int. Ed. Engl1978, 17, 569.
  2. Ryan P. Wurz . Chem. Rev. 2007107, 5570. 
  3. D. V. Evdokimov, N. A. Bumagin. Russ. Chem. Bull. 2007, 56, 1093.
  4. Wilson, S.R.; Augelli, C.E. Org. Synth1990, 68, 210.
  5. Rezgui, F.; El Gaied, M. M. Tetrahedron Lett1998, 39, 5965.

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