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044854

044854-25ml



Isopropylmagnesium chloride lithium chloride 1.3M solution in THF


CAS Number: 745038-86-2
   
Molecular Formula: C3H7MgCl2Li
   
Molecular Weight: 145.25
   
MDL Number: MFCD07784514

Special Handling and Safety: Over 25g Special DOT packaging Charge $20

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044854-25ml
Regular Price: $21.00
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044854-100ml
Regular Price: $64.00
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044854-800ml
Regular Price: $239.00
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044854-2L
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Density:0.951
 
Pictograms:
Signal Word:Danger
Hazard Statements:H225, H314, H335, H351, EUH014, EUH019
Precautionary Statements:P201, P202, P210, P233, P240, P261, P271, P280, P301 + P330 + P331, P303 + P361 + P353, P304 + P340, P305 + P351 + P338, P308 + P313, P403 + P235
UN#:UN3399
Packing Group:II
Hazard Class:4.3
, 3

Flash Point:-17°
SDS: See MSDS
 
Excepted Quantities:Max Inner Pack (30g or 30ml) and Max Outer Pack (500g or 500ml)

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A reagent commonly used with CH3MgCl/LiCl to affect magnesium-halogen exchange on unprotected aryl carboxylic acids.1 Applied for preparing reactive organometallic reagents such as TurboGrignards to increase both the rate and the efficiency of Mg-halogen exchange reaction.2 Used to prepare various functionalized aryl boronic esters derived from hexylene glycol and pinacol,3 functionalize pyridine N-Oxides via iodine or bromine-magnesium exchange,4 allow a sequential 2,3-difunctionalization of various 2-arylsulfinyl furans, thiophenes and benzofurans with TMPMgCl·LiCl (TMP = 2,2,6,6-tetramethylpiperidyl).5

Reference

1.        Chem. Commun. (Camb.)2007, 2075. 
2.        Angew. Chem. Int. Ed. 200443, 3333. 
3.        Org. Process Res. Dev. 201115, 710. 
4.        J. Org. Chem. 200974, 939.
5.        Chem. Commun. (Camb.)  200924, 3536.

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